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Flowchart of the analytical procedures for nitrofuran (NF) metabolites in sausage casing and crawfish, involving washing, derivatization, and LLE steps, coupled with LC-Q-Orbitrap HRMS.

Journal: Toxicology Reports

Article Title: Determination of nitrofuran metabolites in sausage casings and crawfish using LC-Q-Orbitrap HRMS: Method development and validation

doi: 10.1016/j.toxrep.2025.102076

Figure Lengend Snippet: Flowchart of the analytical procedures for nitrofuran (NF) metabolites in sausage casing and crawfish, involving washing, derivatization, and LLE steps, coupled with LC-Q-Orbitrap HRMS.

Article Snippet: Mass spectrometric analysis was conducted employing a Q-Exactive Orbitrap mass spectrometer (Thermo Scientific, Bremen, Germany), which was equipped with a heated electrospray ionization (HESI) source operating in positive ionization mode.

Techniques: